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. 2007 Dec 6;64(Pt 1):o158. doi: 10.1107/S1600536807063076
Bruker X8 Proteum diffractometer 1972 independent reflections
Radiation source: fine-focus rotating anode 1893 reflections with I > 2σ(I)
Monochromator: graded multilayer optics Rint = 0.039
Detector resolution: 18 pixels mm-1 θmax = 69.4º
T = 90.0(2) K θmin = 5.2º
φ and ω scans h = −10→10
Absorption correction: multi-scan(SADABS in APEX2; Bruker, 2006) k = −10→10
Tmin = 0.837, Tmax = 0.944 l = −17→17
15160 measured reflections