Bruker X8 Proteum diffractometer | 1972 independent reflections |
Radiation source: fine-focus rotating anode | 1893 reflections with I > 2σ(I) |
Monochromator: graded multilayer optics | Rint = 0.039 |
Detector resolution: 18 pixels mm-1 | θmax = 69.4º |
T = 90.0(2) K | θmin = 5.2º |
φ and ω scans | h = −10→10 |
Absorption correction: multi-scan(SADABS in APEX2; Bruker, 2006) | k = −10→10 |
Tmin = 0.837, Tmax = 0.944 | l = −17→17 |
15160 measured reflections |