Rigaku Saturn CCD diffractometer | 4526 independent reflections |
Radiation source: Rotating anode | 3651 reflections with I > 2σ(I) |
Monochromator: confocal | Rint = 0.044 |
Detector resolution: 7.31 pixels mm-1 | θmax = 27.9º |
T = 113(2) K | θmin = 1.7º |
ω scans | h = −17→17 |
Absorption correction: multi-scan(REQABS; Jacobson, 1998) | k = −12→12 |
Tmin = 0.484, Tmax = 0.739 | l = −21→20 |
17461 measured reflections |