| Bruker SMART CCD area-detector diffractometer | 6429 independent reflections |
| Radiation source: fine-focus sealed tube | 2812 reflections with I > 2σ(I) |
| Monochromator: graphite | Rint = 0.030 |
| T = 298(2) K | θmax = 26.9º |
| ω scans | θmin = 1.7º |
| Absorption correction: multi-scan(SADABS; Bruker, 2000) | h = −13→9 |
| Tmin = 0.982, Tmax = 0.984 | k = −14→15 |
| 9348 measured reflections | l = −14→17 |
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