Oxford Diffraction Xcalibur S CCD diffractometer	1139 independent reflections
Radiation source: Enhance (Mo) X-ray source	695 reflections with I > 2σ(I)
Monochromator: graphite	Rint = 0.019
Detector resolution: 16.0696 pixels mm-1	θmax = 30.0º
T = 298(2) K	θmin = 2.3º
ω and φ scans	h = −5→5
Absorption correction: none	k = −14→14
3076 measured reflections	l = −22→22