Table 1. Data-collection and data-processing parameters for the V. cholerae CheY3 crystal.
Values in parentheses are for the outermost resolution shell.
Space group | R3 |
Unit-cell parameters (Å) | a = b = 67.98, c = 75.73 |
Rotation range per image (°) | 0.5 |
Resolution range (Å) | 30–1.86 (1.93–1.86) |
No. of molecules per asymmetric unit | 1 |
Matthews coefficient (VM; Å3 Da−1) | 2.33 |
Solvent content (%) | 47 |
No. of observations | 17473 (1566) |
No. of unique reflections | 10370 (985) |
Mosaicity (°) | 0.2 |
Completeness (%) | 94.3 (89.3) |
Redundancy | 1.7 (1.59) |
Rmerge† (%) | 2.25 (7.99) |
B factor (Wilson plot; Å2) | 18.88 |
Average I/σ(I) | 9.7 (5.4) |
R
merge =
, where I
i(hkl) is the observed intensity of the ith measurement of reflection hkl and 〈I(hkl)〉 is the mean intensity of reflection hkl calculated after scaling.