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(a) Anion-exchange FPLC chromatogram of the crude Ru(p-cymene)-HPhen1 reaction mixture. Product eluted at 0.2–0.25 M NaCl using a linear NaCl gradient (0–0.5 M in 10 mM sodium phosphate, pH 8.0). (b) MALDI mass spectra of the major FPLC product identified as the Ru(p-cymene)-HPhen1 complex.
