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. Author manuscript; available in PMC: 2011 Aug 18.
Published in final edited form as: J Am Chem Soc. 2010 Aug 18;132(32):11179–11182. doi: 10.1021/ja103551x

Table 2.

Fe-Mediated Cyclocarbonylation

Entry Vinylcyclopropane Cyclohexenone Yield(%)a,b
1 graphic file with name nihms-224884-t0016.jpg graphic file with name nihms-224884-t0017.jpg 81
2 graphic file with name nihms-224884-t0018.jpg graphic file with name nihms-224884-t0019.jpg 80
3 graphic file with name nihms-224884-t0020.jpg graphic file with name nihms-224884-t0021.jpg 90
4 graphic file with name nihms-224884-t0022.jpg graphic file with name nihms-224884-t0023.jpg 80
5 graphic file with name nihms-224884-t0024.jpg graphic file with name nihms-224884-t0025.jpg 56
6 graphic file with name nihms-224884-t0026.jpg graphic file with name nihms-224884-t0027.jpg 59
a

Yields are for pure chromatographed material.

b

Reactions were run to 52-82% conversion. Yields are based on starting material not recovered.