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. 2010 Jul 26;107(32):13997–14002. doi: 10.1073/pnas.1003009107

Fig. 2.

Fig. 2.

NMR spectra of as-synthesized ITQ-40: 99 MHz 1H-to-29Si CPMAS (Bottom) and 29Si MAS (Bloch decay, Top). (Inset) An overlay of the CPMAS and MAS-NMR spectra. About 9.6% of the total signal in the MAS spectrum is in a region where silanol species are observed. These regions are preferentially enhanced in the CPMAS spectrum.