Fig. 2.
NMR spectra of as-synthesized ITQ-40: 99 MHz 1H-to-29Si CPMAS (Bottom) and 29Si MAS (Bloch decay, Top). (Inset) An overlay of the CPMAS and MAS-NMR spectra. About 9.6% of the total signal in the MAS spectrum is in a region where silanol species are observed. These regions are preferentially enhanced in the CPMAS spectrum.