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. Author manuscript; available in PMC: 2011 Aug 18.
Published in final edited form as: J Am Chem Soc. 2010 Aug 18;132(32):10973–10975. doi: 10.1021/ja103805s

Figure 2.

Figure 2

31P{1H} NMR for A.) neat TOPSe with 15% (mol,mol) DPP and B.) 30 minutes after combining with Pb(oleate)2 at 40 °C. The major products from this reaction (3 (98.9 ppm) and 12 (-14.5 ppm)) are consistent with a reaction between sec-phosphine chalcogenides and metal carboxylates.