Figure 3.
Preparation of diaryliodonium salts 2-7. a) NaBO3, AcOH, 40 °C, 8 h; b) TsOH·H2O, anisole, CH3CN; c) H2O, NaPF6; d) Pd2(dba)3, P(t-Bu)3, benzene, Sn2Bu6, 100 °C; e) p-(OMe)PhI(OTs)(OH), CH3CN.
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