Table 1.
Initial ligand screen for reductive carboxylation
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---|---|---|---|
entry | R | additive | yield (%) |
1 | CO2Me (a) | none | <5 |
2 | CO2Me (a) | bipy | NR |
3 | CO2Me (a) | DBU | 88 |
4 | CO2Me (a) | pyridine | 90 |
5 | CO2Me (a) | PPh3 | NR |
6 | H (b) | DBU | NR |
7 | H (b) | KHMDS | 35 |
8 | H (b) | Cs2CO3 | 56 |