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. Author manuscript; available in PMC: 2010 Sep 2.
Published in final edited form as: Chem Biol. 2009 Jun 26;16(6):667–675. doi: 10.1016/j.chembiol.2009.04.011

Table 2.

Crystallographic Analysis

MAT MT

PDB ID 2JFD 2C2N
Space group P212121 P21
Unit cell a=85.98 Å, b=92.69 Å, c=159.87 Å a=52.57 Å, b=84.83 Å, c=74.56 Å, β=93.43°
Resolution 2.81 Å (2.90 Å − 2.81 Å) 1.55 Å (1.65 Å − 1.55 Å)
Completeness 98.4% (90.5%) 99.4% (96.5%)
Redundancy 4.0 (3.4) 4.0 (2.4)
I/σ(I) 15.8 (2.4) 12.5 (2.3)
Rint 0.050 (0.410) 0.080 (0.280)
Number of atoms 11392 5479
Number of unique reflections 39706 92079
Rwork 0.212 0.178
Rfree 0.273 0.218
R.m.s.d bond lengths 0.011 Å 0.016 Å
R.m.s.d bond angles 1.23° 1.65°

Values in parentheses are for data in highest resolution shell.