Table 1.
Data collection and refinement statistics
| Data collection | |
| Beamline | APS 22-ID |
| Space group | P212121 |
| Wavelength | 0.9792 |
| Unit-cell parameters | 59.408, 73.934, 162.382 |
| Unique reflections | 28453 |
| Completeness (%) | 99.2 (94.7) |
| Resolution (Å) | 2.4 (2.49–2.40) |
| Rmerge (%) | 10.0 (44.7) |
| Redundancy | 3.2 (2.5) |
| I/σ(I) | 11.4 (2.04) |
| Refinement | |
| Resolution Limits (Å) | 20.0–2.40 |
| # reflections/# to compute Rfree | 24660/2000 |
| R (Rfree) | 19.8 (24.9) |
| # protein residues | 579 |
| # solvent molecules | 197 |
| # phosphate molecules | 2 |
| Ramachandran | |
| Most favored | 93.3 |
| Add. allowed | 6.3 |
| Generously | 0.4 |
| Disallowed | 0.0 |
| RMS deviation | |
| Bond, Å | 0.006 |
| Angle, ° | 0.997 |