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. 2010 Aug 31;66(Pt 9):1127–1129. doi: 10.1107/S1744309110030228

Table 1. Data-collection statistics for rATX crystals.

Values in parentheses are for the highest resolution shell.

Crystal data  
 No. of crystals 1
 Beamline APS 23-ID-D
 Detector MAR Mosaic 300
 Total rotation/rotation per frame (°) 460/1
 Space group P1
 Unit-cell parameters (Å, °) a = 53.8, b = 63.3, c = 70.5, α = 98.8, β = 106.2, γ = 99.8
Data collection  
 Wavelength (Å) 1.28299
 Mosaicity (°) 0.4
 Resolution (Å) 20.0–2.05 (2.12–2.05)
 Total No. of reflections 511856
 No. of unique data 52153
 Multiplicity 4.8 (3.0)
 Data completeness (%) 96.8 (93.9)
 Average I/σ(I) 13.9 (2.49)
Rmerge 0.097 (0.378)
 Molecules per asymmetric unit 1
 Matthews coefficient (Å3 Da−1) 2.3
 Solvent content (%) 47

This value includes measurements of partial reflections.

R merge = Inline graphic Inline graphic.