Table 1. Crystallographic parameters: data collection and refinement statistics (for high resolution bin, statistics are given in parentheses).
| Data Collection | |
| Resolution (Å) | 1.50 |
| Space group | C2 |
| Unit cell parameters | |
| a (Å) | 134.35 |
| b (Å) | 38.14 |
| c (Å) | 95.16 |
| β (°) | 114.36 |
| Wavelength (Å) | 0.98 |
| Temperature (K) | 103 |
| Total number reflections | 374500 |
| Total unique reflections | 70666 |
| Completeness | 99.2 (99.7) |
| Redundancy | 5.3 (5.4) |
| Rsym | 0.057 (0.182) |
| I/σI | 19.3 (8.9) |
| Refinement | |
| Resolution range (Å) | 45.31 – 1.50 (1.54 -1.50) |
| Rfactor | 0.122 (0.121) |
| Rfree | 0.158 (0.181) |
| Average B factor (Å2) | |
| ethylene glycol | 26.50 |
| inhibitor | 13.08 |
| protein | 10.01 |
| sulfate | 32.60 |
| water | 24.00 |
| R.m.s deviation from ideal | |
| Bond lengths (Å) | 0.017 |
| Bond angles (°) | 1.76 |
| Ramachandran analysis (MolProbity) | |
| Residues in favored regions (%) | 97.9 |
| Residues in allowed regions (%) | 100 |
| Residues in disallowed regions (%) | 0 |
| Molprobity | |
| Score | 2.48 |
| Percentile | 99% |
| PDB ID | 3LXS |