. Author manuscript; available in PMC: 2011 Oct 13.

Published in final edited form as: Carbohydr Res. 2010 Aug 21;345(15):2228–2232. doi: 10.1016/j.carres.2010.08.011

Table 1.

¹H and ¹³C chemical shifts of HS precursors in D₂O in 37 °C^a

Position ^b	¹H Chemical Shift (ppm)	¹³C Chemical Shift (ppm)
A1	5.58	100.30
A2	3.24	60.77
A3	3.65	72.48
A4	3.65	81.11
A5	3.75	73.61
A6	3.84/3.79	62.65
G1	4.52	105.33
G2	3.38	75.83
G3	3.80	79.96
G4	3.89	78.70
G5	3.82	79.06
G6	-	176.85

Chemical shifts are given in ppm, ¹H chemical shifts is measured indirectly with reference to DSS in D₂O at 25°C. ¹³C is measured indirectly with reference to ¹H using a chemical shift ratio of 0.25144.

A represents glucosamine and G represents glucuronic acid. The numerical suffix corresponds to the carbon position starting with the anomeric carbon as 1.