Table 3.
Protein | HoloCotA | apoCu(I) |
---|---|---|
Beam line at ESRF | ID23-2 | ID23-1 |
Wavelength (Å) | 0.87260 | 0.97625 |
Detector Distance (mm) | 196.4 | 288.17 |
Resolution (Å) | 1.8 | 2.0 |
Space group | P3121 | P3121 |
Cell parameters (Å), a | 101.4 | 101.3 |
c | 137.3 | 136.1 |
Mosaicity (°) | 0.43 | 0.32 |
Oscillation range (°) | 0.8 | 0.45 |
Oscillation angle (°) | 80° | 81° |
No. of unique hkl | 76099 (10995) | 54422 (7901) |
Completeness (%) | 99.9 (100.0) | 99.0 (99.7) |
I/σ(I) | 6.4 (2.4) | 6.6 (2.0) |
Rsymm | 0.071 (0.311) | 0.073 (0.384) |
Multiplicity | 5.0 (5.0) | 4.9 (4.9) |
† Values in parentheses refer to the highest resolution shells as follows;
holoCotA (1.9 Å - 1.80 Å)
ApoCu(I) (2.11 Å - 2.0 Å)