Skip to main content
. Author manuscript; available in PMC: 2011 Oct 1.
Published in final edited form as: Org Lett. 2010 Oct 1;12(19):4384–4387. doi: 10.1021/ol101865e

Table 1.

Pd-Mediated Cross-Coupling of 6a with Various Aryl Chlorides

graphic file with name nihms-235904-f0005.jpg
entry producta yield
1 graphic file with name nihms-235904-t0006.jpg
2 graphic file with name nihms-235904-t0007.jpg
3 graphic file with name nihms-235904-t0008.jpg
4 graphic file with name nihms-235904-t0009.jpg
5 graphic file with name nihms-235904-t0010.jpg
6 graphic file with name nihms-235904-t0011.jpg
7 graphic file with name nihms-235904-t0012.jpg
8 graphic file with name nihms-235904-t0013.jpg
9 graphic file with name nihms-235904-t0014.jpg
10 graphic file with name nihms-235904-t0015.jpg
11 graphic file with name nihms-235904-t0016.jpg
12 graphic file with name nihms-235904-t0017.jpg
a

5% Pd(OAc)2, 10% RuPhos, 3 equiv K2CO3, toluene/H2O, 85 °C, 22 h

b 5% Pd(OAc)2, 10% SPhos, 3 equiv K2CO3, toluene/H2O, 85 °C, 22 h