Table 1. Summary of crystallographic analysis.
Resolution, Å | 30.0-2.3 (2.4-2.3) |
Wavelength, Å | 1.033 |
Completeness, % | 99.9 (99.8) |
Redundancy, fold | 7.5 (5.9) |
I/σI | 22.8 (3.6) |
Rmerge, % | 11.5 (46.4) |
Space Group | P212121 |
Cell Dimensions, Å | a=43.09, b=62.33, c=135.93 |
Refinement | |
Reflections working / test | 18002 / 980 |
Residues | 360 |
Solvent | 240 |
Rcrys/Rfree | 19.8/28.5 (22.3/32.3) |
R.m.s. deviations | |
Bonds, Å | 0.019 |
Angles, ° | 1.80 |
Ramachandran Analysis | |
Most favored regions | 92.4 % |
Values in parentheses correspond to the high-resolution shell.
Rmerge = Σ|I−<I>|/ΣI, where I = observed intensity and <I> = average intensity obtained from multiple observations of symmetry-related reflections.
The r.m.s. deviations in bond lengths and angles are the respective root-mean-square deviations from ideal values