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. Author manuscript; available in PMC: 2011 Oct 13.
Published in final edited form as: J Am Chem Soc. 2010 Oct 13;132(40):14137–14151. doi: 10.1021/ja105044s

Table 5.

C–H olefination of 1 using 0.2 mol% Pd(OAc)2 and 1 atm O2.a

graphic file with name nihms-238338-t0011.jpg

Entry Time (h) % Conv.
1 0 0
2 4 15
3 20 52
4 48 91 (83)
a

The conversion was determined by 1H NMR analysis of the crude reaction mixture.