Table 1.
Crystal data and structure refinement for complex 1.
| Empirical formula | C26H34Cd2N2O12 |
| Formula weight | 791.35 |
| Crystal size (mm) | 0.20 × 0.23 × 0.50 |
| Crystal system | Tetragonal |
| Space group | P41212 |
| Flack parameter x | 0.01(3) |
| θ range for data collection (°) | 1.95 ≤ θ ≤ 25.04 |
| a, Å | 12.737(5) |
| b, Å | 12.737(5) |
| c, Å | 18.288(7) |
| α° | 90 |
| β° | 90 |
| γ° | 90 |
| V, Å3 | 2967(2) |
| Z | 4 |
| ρ calcd, g cm−3 | 1.772 |
| μ, mm−1 | 1.498 |
| F(000) | 1584 |
| Limiting indices, (°) | 0 ≤ h ≤ 15 |
| 0 ≤ k ≤ 15 | |
| −21 ≤ l ≤ 21 | |
| Reflections collected | 5741 |
| Unique reflections | 2632 (R int = 0.0454) |
| Reflections used [I > 2σ(I)] | 2448 |
| Parameters | 246 |
| GoF (on F 2) | 1.047 |
| R1a | 0.0273 |
| w R2a | 0.0674 |
| (Δρ)max /(Δρ)min , e Å−3 | 0.742/−0.570 |
a I > 2σ(I).