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. Author manuscript; available in PMC: 2011 Oct 13.
Published in final edited form as: J Am Chem Soc. 2010 Oct 13;132(40):14092–14103. doi: 10.1021/ja1036644

Figure 1.

Figure 1

Synthesis of 1. ORTEP drawing of 9 and 1 with ellipsoids drawn at 50% probability (hydrogen atoms omitted for clarity). Selected bond lengths in 1 [Å]: Pd(1A)–Pd(1B), 2.5672(5); Pd(1A)–Cl(A), 2.4167(10); Pd(1A)–C(A), 2.000(4); Pd(1A)–O(1A), 2.133(3); Pd(1A)–O(2A), 2.042(3); Pd(1A)–N(A), 2.016(3). For comparison, the Pd–Pd distance in 9 is: 2.8419(8) Å.