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. Author manuscript; available in PMC: 2011 Sep 24.
Published in final edited form as: J Nat Prod. 2010 Sep 24;73(9):1553–1558. doi: 10.1021/np100406d

Table 2.

13C NMR Spectroscopic Data of 16

position δC, mult.

1 a 2 a 3 b 4 a 5 b 6 b
1 83.0 CH 83.1 CH 84.7 CH 83.0 CH 83.6 CH 83.9 CH
2 196.0 qC 196.0 qC 197.6 qC 196.0 qC 72.9 CH 73.0 CH
3 124.2 CH 124.1 CH 126.5 CH 124.3 CH 126.8 CH 127.3 CH
4 164.7 qC 165.1 qC 162.7 qC 164.7 qC 134.9 qC 135.2 qC
5 41.7 CH 41.7 CH 42.5 CH 41.7 CH 41.4 CH 42.3 CH
6 25.4 CH2 25.3 CH2 26.2 CH2 25.5 CH2 25.7 CH2 26.2 CH2
7 77.3 CH 77.2 CH 78.7 CH 77.3 CH 78.8 CH 79.3 CH
8 47.5 qC 47.4 qC 46.5 qC 47.3 qC 48.1 qC 46.4 qC
9 44.4 CH 44.2 CH 45.9 CH 44.5 CH 45.1 CH 45.7 CH
10 45.3 qC 45.3 qC 45.7 qC 45.2 qC 42.1 qC 41.7 qC
11 108.8 qC 108.7 qC 111.0 qC 108.9 qC 110.7 qC 111.3 qC
12 79.3 CH 79.5 CH 80.3 CH 79.2 CH 80.2 CH 80.4 CH
13 31.4 CH 31.2 CH 33.0 CH 31.4 CH 32.7 CH 33.3 CH
14 45.5 CH 44.8 CH 48.4 CH 45.6 CH 45.7 CH 48.4 CH
15 71.0 CH 71.0 CH 71.8 CH 69.4 CH 73.0 CH 70.6 CH
16 167.0 qC 167.0 qC 168.4 qC 167.3 qC 167.7 qC 168.7 qC
18 23.0 CH3 23.0 CH3 22.6 CH3 23.0 CH3 21.0 CH3 21.5 CH3
19 10.1 CH3 10.1 CH3 11.2 CH3 10.0 CH3 11.0 CH3 11.3 CH3
20 71.0 CH2 71.9 CH2 71.6 CH2 71.0 CH2 71.4 CH2 71.9 CH2
21 14.1 CH3 14.1 CH3 16.1 CH3 14.5 CH3 15.6 CH3 15.9 CH3
1′ 171.4 qC 171.4 qC 176.7 qC 175.7 qC 171.4 qC 175.8 qC
2′ 80.7 qC 80.6 qC 75.6 qC 41.0 CH 81.1 qC 41.9 CH
3′ 30.1 CH2 31.7 CH2 34.2 CH2 26.5 CH2 31.4 CH2 27.4 CH2
4′ 7.2 CH3 7.2 CH3 8.8 CH3 11.5 CH3 7.5 CH3 12.2 CH3
5′ 21.1 CH3 21.1 CH3 26.1 CH3 16.0 CH3 21.0 CH3 16.5 CH3
1″ 170.1 qC 170.3 qC 169.9 qC
2″ 20.9 CH3 20.3 CH3 21.0 CH3
a

Measured in CDCl3;

b

Measured in pyridine-d5