Table 3.
DSC parameters of GTCC and CoQ10 in the bulk GTCC, CoQ10 and CoQ10-LNCs 3 days after being produced for three cycles at 300 bar/600 bar/1000 bar, respectively
| Formulation | GTCC | CoQ10 | ||||||
|---|---|---|---|---|---|---|---|---|
| Melting point (°C) | Onset (°C) | Enthalpy (J/g) | CI% | Melting point (°C) | Onset (°C) | Enthalpy (J/g) | CI% | |
| GTCC | −2.92 | −11.57 | 95.63 | 100 | / | / | / | / |
| CoQ10 | / | / | / | / | 49.12 | 47.76 | 131.2 | 100 |
| 100-0 bar | / | / | / | / | 48.11 | 45.19 | 16.75 | 95.77 |
| 100-300 bar | / | / | / | / | 47.84 | 45.53 | 0.3388 | 1.94 |
| 75-0 bar | −3.69 | −10.29 | 2.21 | 69.27 | 45.16 | 39.41 | 11.16 | 85.06 |
| 75-300 bar | / | / | / | / | 44.72 | 38.94 | 0.2943 | 2.24 |
| 50-0 bar | −4.03 | −12.53 | 4.29 | 67.32 | 40.72 | 32.61 | 6.787 | 77.56 |
| 50-300 bar | −11 | −35.19 | 4.19 | 65.67 | 39.54 | 31.93 | 0.2208 | 2.52 |
| 50-600 bar | −23.05 | −40.19 | 4.03 | 63.18 | / | / | / | / |
| 50-1000 bar | −23.2 | −40.76 | 4.09 | 64.12 | / | / | / | / |
| 25-0 bar | −4.08 | −11.96 | 8.57 | 89.61 | 34.41 | 26.35 | 3.011 | 68.91 |
| 25-300 bar | −6.11 | −29.92 | 6.63 | 69.29 | 34.44 | 26.15 | 0.1216 | 2.78 |
| 25-600 bar | −11.92 | −19.84 | 5.39 | 56.37 | / | / | / | / |
| 25-1000 bar | −11.61 | −19.73 | 5.38 | 56.31 | / | / | / | / |
| 0-0 bar | −3.05 | −10.18 | 12.01 | 94.21 | / | / | / | / |
| 0-300 bar | −3.44 | −18.24 | 9.69 | 75.99 | / | / | / | / |
| 0-600 bar | −9.23 | −16.35 | 9.28 | 72.78 | / | / | / | / |
| 0-1000 bar | −8.69 | −16.12 | 9.17 | 71.67 | / | / | / | / |