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. Author manuscript; available in PMC: 2011 Aug 1.
Published in final edited form as: J Struct Biol. 2010 Apr 4;171(2):231–237. doi: 10.1016/j.jsb.2010.03.020

Table 1. X-ray Data Collection Statistics on RCK Crystals.

Data 5 mM Cd 10 mM Ca Native
Space group p21 p21 p21
Unit cell dimensions (a, b, c in Å, angles in °) 58.02, 38.29, 96.63, 90.00, 95.10, 90.00 58.136, 38.31, 96, 88, 90.00, 95.28, 90.00 58.44, 38.33, 96.92, 90.00, 94.88, 90.00
Resolution in Å 57.8 - 2.2 (2.32 - 2.2) 57-9 - 2.3 (2.42 - 2.3) 58.22 - 2.0 (2.11 - 2.00)
Wilson B-factor 36.3 33.9 25.9
reflections observed 80, 630 (11, 993) 71, 400 (10, 564) 111, 034 (16, 475)
unique reflections 21, 805 (3, 163) 19, 216 (2, 789) 29, 003 (4, 198)
% Completeness 99.4 (99.1) 99.5 (99.8) 98.6 (98.5)
Multiplicity 3.7 (3.8) 3.7 (3.8) 3.8 (3.9)
Mean((I)/σ(I)) 10.8 (4.7) 10.4 (6.6) 12.0 (6.7)
Rsym # 0.039 (0.159) 0.044 (0.104) 0.035 (0.107)

*Parenthesis refer to highest resolution shell

hklΣi∣Ii(hkl) - <I(hkl)> ∣ / ΣhΣiIi(hkl), where Ii(hkl) is the ith measurement and <I(hkl)> is the mean of all measurements of I(hkl) for Miller indices hkl.