Table 1. X-ray Data Collection Statistics on RCK Crystals.
Data | 5 mM Cd | 10 mM Ca | Native |
Space group | p21 | p21 | p21 |
Unit cell dimensions (a, b, c in Å, angles in °) | 58.02, 38.29, 96.63, 90.00, 95.10, 90.00 | 58.136, 38.31, 96, 88, 90.00, 95.28, 90.00 | 58.44, 38.33, 96.92, 90.00, 94.88, 90.00 |
Resolution in Å | 57.8 - 2.2 (2.32 - 2.2) | 57-9 - 2.3 (2.42 - 2.3) | 58.22 - 2.0 (2.11 - 2.00) |
Wilson B-factor | 36.3 | 33.9 | 25.9 |
reflections observed | 80, 630 (11, 993) | 71, 400 (10, 564) | 111, 034 (16, 475) |
unique reflections | 21, 805 (3, 163) | 19, 216 (2, 789) | 29, 003 (4, 198) |
% Completeness | 99.4 (99.1) | 99.5 (99.8) | 98.6 (98.5) |
Multiplicity | 3.7 (3.8) | 3.7 (3.8) | 3.8 (3.9) |
Mean((I)/σ(I)) | 10.8 (4.7) | 10.4 (6.6) | 12.0 (6.7) |
Rsym # | 0.039 (0.159) | 0.044 (0.104) | 0.035 (0.107) |
*Parenthesis refer to highest resolution shell
#ΣhklΣi∣Ii(hkl) - <I(hkl)> ∣ / ΣhΣiIi(hkl), where Ii(hkl) is the ith measurement and <I(hkl)> is the mean of all measurements of I(hkl) for Miller indices hkl.