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. 2008 Sep 20;64(Pt 10):o1961–o1962. doi: 10.1107/S1600536808029218
O2A—C8A 1.229 (5) O2B—C8B 1.237 (5)
N1A—C7A 1.296 (5) N1B—C7B 1.292 (5)
N1A—N2A 1.388 (4) N1B—N2B 1.389 (4)
N2A—C8A 1.351 (5) N2B—C8B 1.356 (5)
N2A—H2NA 0.9145 N2B—H2NB 0.7271
C1A—C2A 1.385 (5) C1B—C2B 1.384 (5)
C1A—C6A 1.406 (5) C1B—C6B 1.397 (5)
C1A—H1AA 0.9300 C1B—H1BA 0.9300
C2A—C3A 1.385 (6) C2B—C3B 1.395 (6)
C2A—H2AA 0.9300 C2B—H2BA 0.9300
C3A—C4A 1.392 (6) C3B—C4B 1.387 (5)
C3A—H3AA 0.9300 C3B—H3BA 0.9300
C4A—C5A 1.382 (5) C4B—C5B 1.381 (5)
C4A—H4AA 0.9300 C4B—H4BA 0.9300
C5A—C6A 1.400 (5) C5B—C6B 1.404 (5)
C5A—H5AA 0.9300 C5B—H5BA 0.9300
C6A—C7A 1.492 (5) C6B—C7B 1.495 (5)
C7A—C15A 1.491 (5) C7B—C15B 1.498 (5)
C8A—C9A 1.499 (5) C8B—C9B 1.509 (5)
C9A—C10A 1.396 (5) C9B—C14B 1.382 (5)
C9A—C14A 1.399 (5) C9B—C10B 1.406 (5)
C10A—C11A 1.388 (6) C10B—C11B 1.384 (6)
C10A—H10A 0.9300 C10B—H10B 0.9300
C11A—C12A 1.385 (6) C11B—C12B 1.389 (6)
C11A—H11A 0.9300 C11B—H11B 0.9300
C12A—C13A 1.386 (6) C12B—C13B 1.387 (6)
C12A—H12A 0.9300 C12B—H12B 0.9300
C13A—C14A 1.385 (5) C13B—C14B 1.401 (5)
C13A—H13A 0.9300 C13B—H13B 0.9300
C14A—H14A 0.9300 C14B—H14B 0.9300
C15A—H15A 0.9600 C15B—H15D 0.9600
C15A—H15B 0.9600 C15B—H15E 0.9600
C15A—H15C 0.9600 C15B—H15F 0.9600
C7A—N1A—N2A 117.0 (3) C7B—N1B—N2B 117.1 (3)
C8A—N2A—N1A 116.6 (3) C8B—N2B—N1B 116.1 (3)
C8A—N2A—H2NA 120.6 C8B—N2B—H2NB 114.2
N1A—N2A—H2NA 117.0 N1B—N2B—H2NB 129.5
C2A—C1A—C6A 120.7 (4) C2B—C1B—C6B 120.5 (4)
C2A—C1A—H1AA 119.6 C2B—C1B—H1BA 119.8
C6A—C1A—H1AA 119.6 C6B—C1B—H1BA 119.8
C3A—C2A—C1A 120.5 (4) C1B—C2B—C3B 120.2 (4)
C3A—C2A—H2AA 119.7 C1B—C2B—H2BA 119.9
C1A—C2A—H2AA 119.7 C3B—C2B—H2BA 119.9
C2A—C3A—C4A 119.5 (4) C4B—C3B—C2B 119.7 (4)
C2A—C3A—H3AA 120.3 C4B—C3B—H3BA 120.1
C4A—C3A—H3AA 120.3 C2B—C3B—H3BA 120.1
C5A—C4A—C3A 120.2 (4) C5B—C4B—C3B 120.2 (4)
C5A—C4A—H4AA 119.9 C5B—C4B—H4BA 119.9
C3A—C4A—H4AA 119.9 C3B—C4B—H4BA 119.9
C4A—C5A—C6A 121.1 (4) C4B—C5B—C6B 120.6 (3)
C4A—C5A—H5AA 119.4 C4B—C5B—H5BA 119.7
C6A—C5A—H5AA 119.4 C6B—C5B—H5BA 119.7
C5A—C6A—C1A 117.9 (3) C1B—C6B—C5B 118.8 (3)
C5A—C6A—C7A 121.1 (3) C1B—C6B—C7B 120.6 (3)
C1A—C6A—C7A 121.0 (3) C5B—C6B—C7B 120.6 (3)
N1A—C7A—C15A 126.3 (3) N1B—C7B—C6B 114.5 (3)
N1A—C7A—C6A 114.3 (3) N1B—C7B—C15B 126.2 (3)
C15A—C7A—C6A 119.4 (3) C6B—C7B—C15B 119.2 (3)
O2A—C8A—N2A 122.4 (3) O2B—C8B—N2B 122.6 (3)
O2A—C8A—C9A 119.5 (3) O2B—C8B—C9B 119.3 (3)
N2A—C8A—C9A 118.1 (3) N2B—C8B—C9B 118.1 (3)
C10A—C9A—C14A 119.2 (3) C14B—C9B—C10B 119.7 (4)
C10A—C9A—C8A 116.7 (3) C14B—C9B—C8B 123.3 (3)
C14A—C9A—C8A 124.1 (3) C10B—C9B—C8B 116.9 (3)
C11A—C10A—C9A 120.2 (4) C11B—C10B—C9B 119.8 (4)
C11A—C10A—H10A 119.9 C11B—C10B—H10B 120.1
C9A—C10A—H10A 119.9 C9B—C10B—H10B 120.1
C12A—C11A—C10A 120.2 (4) C10B—C11B—C12B 120.3 (4)
C12A—C11A—H11A 119.9 C10B—C11B—H11B 119.9
C10A—C11A—H11A 119.9 C12B—C11B—H11B 119.9
C11A—C12A—C13A 119.7 (4) C13B—C12B—C11B 120.4 (4)
C11A—C12A—H12A 120.1 C13B—C12B—H12B 119.8
C13A—C12A—H12A 120.1 C11B—C12B—H12B 119.8
C14A—C13A—C12A 120.6 (4) C12B—C13B—C14B 119.4 (4)
C14A—C13A—H13A 119.7 C12B—C13B—H13B 120.3
C12A—C13A—H13A 119.7 C14B—C13B—H13B 120.3
C13A—C14A—C9A 120.0 (4) C9B—C14B—C13B 120.4 (4)
C13A—C14A—H14A 120.0 C9B—C14B—H14B 119.8
C9A—C14A—H14A 120.0 C13B—C14B—H14B 119.8
C7A—C15A—H15A 109.5 C7B—C15B—H15D 109.5
C7A—C15A—H15B 109.5 C7B—C15B—H15E 109.5
H15A—C15A—H15B 109.5 H15D—C15B—H15E 109.5
C7A—C15A—H15C 109.5 C7B—C15B—H15F 109.5
H15A—C15A—H15C 109.5 H15D—C15B—H15F 109.5
H15B—C15A—H15C 109.5 H15E—C15B—H15F 109.5
C7A—N1A—N2A—C8A 167.6 (3) C7B—N1B—N2B—C8B 166.7 (3)
C6A—C1A—C2A—C3A 0.0 (6) C6B—C1B—C2B—C3B 0.7 (6)
C1A—C2A—C3A—C4A 0.7 (6) C1B—C2B—C3B—C4B −0.3 (6)
C2A—C3A—C4A—C5A −1.0 (6) C2B—C3B—C4B—C5B −0.5 (6)
C3A—C4A—C5A—C6A 0.6 (6) C3B—C4B—C5B—C6B 0.9 (6)
C4A—C5A—C6A—C1A 0.1 (6) C2B—C1B—C6B—C5B −0.3 (6)
C4A—C5A—C6A—C7A −178.3 (3) C2B—C1B—C6B—C7B 178.1 (4)
C2A—C1A—C6A—C5A −0.4 (6) C4B—C5B—C6B—C1B −0.5 (6)
C2A—C1A—C6A—C7A 178.0 (3) C4B—C5B—C6B—C7B −178.9 (4)
N2A—N1A—C7A—C15A −4.2 (6) N2B—N1B—C7B—C6B 174.9 (3)
N2A—N1A—C7A—C6A 176.2 (3) N2B—N1B—C7B—C15B −3.6 (6)
C5A—C6A—C7A—N1A 6.8 (5) C1B—C6B—C7B—N1B −170.8 (3)
C1A—C6A—C7A—N1A −171.5 (3) C5B—C6B—C7B—N1B 7.6 (5)
C5A—C6A—C7A—C15A −172.8 (4) C1B—C6B—C7B—C15B 7.8 (5)
C1A—C6A—C7A—C15A 8.8 (5) C5B—C6B—C7B—C15B −173.8 (3)
N1A—N2A—C8A—O2A −9.0 (5) N1B—N2B—C8B—O2B −8.4 (5)
N1A—N2A—C8A—C9A 174.2 (3) N1B—N2B—C8B—C9B 172.6 (3)
O2A—C8A—C9A—C10A 19.1 (5) O2B—C8B—C9B—C14B −158.2 (4)
N2A—C8A—C9A—C10A −164.0 (3) N2B—C8B—C9B—C14B 20.9 (6)
O2A—C8A—C9A—C14A −158.9 (4) O2B—C8B—C9B—C10B 17.6 (5)
N2A—C8A—C9A—C14A 18.0 (5) N2B—C8B—C9B—C10B −163.3 (3)
C14A—C9A—C10A—C11A 0.6 (6) C14B—C9B—C10B—C11B −1.2 (6)
C8A—C9A—C10A—C11A −177.4 (4) C8B—C9B—C10B—C11B −177.2 (4)
C9A—C10A—C11A—C12A −1.2 (6) C9B—C10B—C11B—C12B 0.0 (6)
C10A—C11A—C12A—C13A 1.4 (6) C10B—C11B—C12B—C13B −0.2 (6)
C11A—C12A—C13A—C14A −1.1 (6) C11B—C12B—C13B—C14B 1.5 (6)
C12A—C13A—C14A—C9A 0.5 (6) C10B—C9B—C14B—C13B 2.6 (6)
C10A—C9A—C14A—C13A −0.3 (6) C8B—C9B—C14B—C13B 178.3 (4)
C8A—C9A—C14A—C13A 177.6 (4) C12B—C13B—C14B—C9B −2.7 (6)