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. 2008 Sep 27;64(Pt 10):m1325. doi: 10.1107/S1600536808030109
Refinement on F2 Primary atom site location: structure-invariant direct methods
Least-squares matrix: full Secondary atom site location: difference Fourier map
R[F2 > 2σ(F2)] = 0.023 Hydrogen site location: inferred from neighbouring sites
wR(F2) = 0.064 H-atom parameters constrained
S = 1.11 w = 1/[σ2(Fo2) + (0.0295P)2 + 15.2156P] where P = (Fo2 + 2Fc2)/3
2850 reflections (Δ/σ)max = 0.002
165 parameters Δρmax = 2.05 e Å3
0 restraints Δρmin = −1.43 e Å3