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. 2008 Sep 20;64(Pt 10):m1298–m1299. doi: 10.1107/S1600536808029140
Refinement on F2 Primary atom site location: structure-invariant direct methods
Least-squares matrix: full Secondary atom site location: difference Fourier map
R[F2 > 2σ(F2)] = 0.039 Hydrogen site location: mixed
wR(F2) = 0.099 H-atom parameters constrained
S = 1.00 w = 1/[σ2(Fo2) + (0.043P)2 + 2.120P] where P = (Fo2 + 2Fc2)/3
6067 reflections (Δ/σ)max = 0.001
382 parameters Δρmax = 0.86 e Å3
0 restraints Δρmin = −0.84 e Å3