Bruker APEXII CCD area-detector diffractometer | 8997 independent reflections |
Radiation source: fine-focus sealed tube | 8334 reflections with I > 2σ(I) |
graphite | Rint = 0.038 |
ω scans | θmax = 33.5°, θmin = 1.7° |
Absorption correction: multi-scan (SADABS; Bruker, 2006) | h = −14→11 |
Tmin = 0.771, Tmax = 0.948 | k = −16→16 |
47170 measured reflections | l = −35→36 |