Table 1. Hydrogen-bond geometry (Å, °).
| D—H⋯A | D—H | H⋯A | D⋯A | D—H⋯A |
|---|---|---|---|---|
| N1—H1A⋯O4i | 0.90 (4) | 2.03 (4) | 2.896 (4) | 161 (3) |
| N1—H1B⋯O1ii | 0.82 (4) | 2.47 (3) | 2.751 (3) | 101 (3) |
| N1—H1B⋯O12 | 0.82 (4) | 2.01 (4) | 2.814 (4) | 168 (3) |
| N1—H1C⋯O11iii | 0.99 (4) | 1.92 (4) | 2.870 (3) | 161 (3) |
| N2—H2A⋯O4iii | 0.82 (4) | 2.07 (4) | 2.801 (4) | 149 (3) |
| N2—H2C⋯O5 | 0.97 (4) | 2.16 (4) | 2.927 (4) | 135 (3) |
| N2—H2B⋯O6 | 0.84 (4) | 2.20 (4) | 2.889 (4) | 139 (3) |
| N2—H2C⋯O3i | 0.97 (4) | 2.19 (4) | 2.940 (3) | 134 (3) |
| O2—H2D⋯O11iv | 0.80 (4) | 1.91 (4) | 2.688 (3) | 164 (4) |
| O3—H3A⋯O1 | 0.86 (4) | 1.77 (4) | 2.569 (3) | 153 (4) |
| O8—H8A⋯O13v | 0.87 (5) | 1.76 (5) | 2.598 (4) | 160 (4) |
| O9—H9A⋯O7 | 0.86 (5) | 1.96 (4) | 2.678 (3) | 141 (4) |
| O9—H9A⋯O6vi | 0.86 (5) | 2.38 (4) | 2.872 (3) | 117 (3) |
| O13—H13A⋯O10vii | 0.83 (8) | 1.93 (8) | 2.759 (4) | 176 (7) |
| O13—H13B⋯O6 | 0.89 (7) | 2.39 (7) | 3.064 (4) | 132 (6) |
| C2—H2⋯O5viii | 0.93 | 2.54 | 3.452 (4) | 168 |
| C6—H6⋯O12 | 0.93 | 2.48 | 3.210 (3) | 136 |
| C12—H12⋯O9ix | 0.93 | 2.55 | 3.428 (4) | 158 |
| C16—H16⋯Cgx | 0.93 | 2.85 | 3.727 (3) | 157 |
Symmetry codes: (i)
; (ii)
; (iii)
; (iv)
; (v)
; (vi)
; (vii)
; (viii)
; (ix)
; (x)
. Cg is the centroid of the C8–C13 ring.