| Bruker SMART APEX CCD area-detector diffractometer | 5262 independent reflections |
| Radiation source: fine-focus sealed tube | 2854 reflections with I > 2σ(I) |
| graphite | Rint = 0.045 |
| ω scans | θmax = 25.5°, θmin = 1.8° |
| Absorption correction: multi-scan (SADABS; Bruker, 2000) | h = −14→14 |
| Tmin = 0.925, Tmax = 0.979 | k = −14→18 |
| 15002 measured reflections | l = −19→20 |
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