| Bruker SMART CCD area-detector diffractometer | 2336 independent reflections |
| Radiation source: fine-focus sealed tube | 2256 reflections with I > 2σ(I) |
| graphite | Rint = 0.027 |
| φ and ω scans | θmax = 25.0°, θmin = 2.0° |
| Absorption correction: multi-scan (SADABS; Sheldrick, 2008) | h = −12→12 |
| Tmin = 0.749, Tmax = 0.849 | k = −10→10 |
| 12799 measured reflections | l = −17→17 |
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