Bruker SMART APEX diffractometer | 2128 independent reflections |
Radiation source: fine-focus sealed tube | 1925 reflections with I > 2σ(I) |
graphite | Rint = 0.034 |
ω scans | θmax = 27.5°, θmin = 2.4° |
Absorption correction: multi-scan (SADABS; Sheldrick, 1996) | h = −23→22 |
Tmin = 0.973, Tmax = 0.991 | k = −6→6 |
4390 measured reflections | l = −15→15 |