| Ni1—C1 | 1.911 (3) | C7—H7C | 0.9700 |
| Ni1—O1i | 1.976 (3) | C8—H8A | 0.9700 |
| Ni1—O1 | 1.976 (3) | C8—H8B | 0.9700 |
| Ni1—P1i | 2.2195 (4) | C8—H8C | 0.9700 |
| Ni1—P1 | 2.2195 (4) | C9—H9A | 0.9700 |
| P1—C5 | 1.831 (2) | C9—H9B | 0.9700 |
| P1—C6 | 1.876 (2) | C9—H9C | 0.9700 |
| P1—C10 | 1.882 (2) | C10—C13 | 1.503 (4) |
| C1—C2i | 1.409 (2) | C10—C12 | 1.516 (6) |
| C1—C2 | 1.409 (2) | C10—C11 | 1.525 (4) |
| C2—C3 | 1.389 (3) | C11—H11A | 0.9700 |
| C2—C5 | 1.501 (3) | C11—H11B | 0.9700 |
| C3—C4 | 1.386 (3) | C11—H11C | 0.9700 |
| C3—H3 | 0.9400 | C12—H12A | 0.9700 |
| C4—C3i | 1.386 (3) | C12—H12B | 0.9700 |
| C4—H4 | 0.9400 | C12—H12C | 0.9700 |
| C5—H5A | 0.9800 | C13—H13A | 0.9700 |
| C5—H5B | 0.9800 | C13—H13B | 0.9700 |
| C6—C9 | 1.521 (3) | C13—H13C | 0.9700 |
| C6—C8 | 1.528 (4) | N1—O3 | 1.223 (5) |
| C6—C7 | 1.541 (3) | N1—O2 | 1.239 (7) |
| C7—H7A | 0.9700 | N1—O1 | 1.273 (5) |
| C7—H7B | 0.9700 | O3—N1i | 1.223 (5) |
| C1—Ni1—O1i | 164.64 (11) | C6—C8—H8B | 109.5 |
| C1—Ni1—O1 | 164.64 (11) | H8A—C8—H8B | 109.5 |
| C1—Ni1—P1i | 84.437 (14) | C6—C8—H8C | 109.5 |
| O1i—Ni1—P1i | 97.74 (10) | H8A—C8—H8C | 109.5 |
| O1—Ni1—P1i | 93.00 (10) | H8B—C8—H8C | 109.5 |
| C1—Ni1—P1 | 84.435 (14) | C6—C9—H9A | 109.5 |
| O1i—Ni1—P1 | 93.00 (10) | C6—C9—H9B | 109.5 |
| O1—Ni1—P1 | 97.74 (10) | H9A—C9—H9B | 109.5 |
| P1i—Ni1—P1 | 168.87 (3) | C6—C9—H9C | 109.5 |
| C5—P1—C6 | 103.63 (10) | H9A—C9—H9C | 109.5 |
| C5—P1—C10 | 105.18 (12) | H9B—C9—H9C | 109.5 |
| C6—P1—C10 | 112.97 (10) | C13—C10—C12 | 110.1 (3) |
| C5—P1—Ni1 | 101.56 (7) | C13—C10—C11 | 108.7 (3) |
| C6—P1—Ni1 | 117.12 (7) | C12—C10—C11 | 106.1 (3) |
| C10—P1—Ni1 | 114.22 (8) | C13—C10—P1 | 113.5 (2) |
| C2i—C1—C2 | 116.2 (3) | C12—C10—P1 | 110.6 (2) |
| C2i—C1—Ni1 | 121.90 (13) | C11—C10—P1 | 107.52 (16) |
| C2—C1—Ni1 | 121.90 (13) | C10—C11—H11A | 109.5 |
| C3—C2—C1 | 121.9 (2) | C10—C11—H11B | 109.5 |
| C3—C2—C5 | 119.73 (18) | H11A—C11—H11B | 109.5 |
| C1—C2—C5 | 118.39 (19) | C10—C11—H11C | 109.5 |
| C4—C3—C2 | 120.4 (2) | H11A—C11—H11C | 109.5 |
| C4—C3—H3 | 119.8 | H11B—C11—H11C | 109.5 |
| C2—C3—H3 | 119.8 | C10—C12—H12A | 109.5 |
| C3i—C4—C3 | 119.3 (3) | C10—C12—H12B | 109.5 |
| C3i—C4—H4 | 120.4 | H12A—C12—H12B | 109.5 |
| C3—C4—H4 | 120.4 | C10—C12—H12C | 109.5 |
| C2—C5—P1 | 106.33 (13) | H12A—C12—H12C | 109.5 |
| C2—C5—H5A | 110.5 | H12B—C12—H12C | 109.5 |
| P1—C5—H5A | 110.5 | C10—C13—H13A | 109.5 |
| C2—C5—H5B | 110.5 | C10—C13—H13B | 109.5 |
| P1—C5—H5B | 110.5 | H13A—C13—H13B | 109.5 |
| H5A—C5—H5B | 108.7 | C10—C13—H13C | 109.5 |
| C9—C6—C8 | 108.4 (2) | H13A—C13—H13C | 109.5 |
| C9—C6—C7 | 109.6 (2) | H13B—C13—H13C | 109.5 |
| C8—C6—C7 | 108.6 (2) | O1i—N1—O3 | 165.1 (6) |
| C9—C6—P1 | 112.18 (18) | O1i—N1—O2 | 64.8 (4) |
| C8—C6—P1 | 104.93 (15) | O3—N1—O2 | 123.0 (4) |
| C7—C6—P1 | 112.90 (16) | O3—N1—O1 | 118.8 (4) |
| C6—C7—H7A | 109.5 | O2—N1—O1 | 117.9 (5) |
| C6—C7—H7B | 109.5 | N1i—O1—O2i | 69.6 (4) |
| H7A—C7—H7B | 109.5 | O2i—O1—N1 | 104.4 (4) |
| C6—C7—H7C | 109.5 | N1i—O1—Ni1 | 152.8 (5) |
| H7A—C7—H7C | 109.5 | O2i—O1—Ni1 | 133.8 (4) |
| H7B—C7—H7C | 109.5 | N1—O1—Ni1 | 121.0 (3) |
| C6—C8—H8A | 109.5 |