Bruker SMART CCD area-detector diffractometer | 2394 independent reflections |
Radiation source: fine-focus sealed tube | 1671 reflections with I > 2σ(I) |
graphite | Rint = 0.058 |
φ and ω scans | θmax = 25.1°, θmin = 1.8° |
Absorption correction: multi-scan (SADABS; Bruker, 2002) | h = −10→10 |
Tmin = 0.965, Tmax = 0.968 | k = −27→26 |
7173 measured reflections | l = −9→9 |