| O1—C1 | 1.2028 (16) | C12—C13 | 1.380 (2) |
| O2—C1 | 1.3475 (17) | C13—C14 | 1.376 (2) |
| O2—C9 | 1.4636 (15) | C14—C15 | 1.383 (2) |
| O3—C13 | 1.3655 (17) | C3—H3 | 0.9300 |
| O3—C16 | 1.418 (2) | C4—H4 | 0.9300 |
| C1—C2 | 1.4741 (19) | C5—H5 | 0.9300 |
| C2—C3 | 1.387 (2) | C6—H6 | 0.9300 |
| C2—C7 | 1.3931 (18) | C8—H8A | 0.9700 |
| C3—C4 | 1.377 (2) | C8—H8B | 0.9700 |
| C4—C5 | 1.375 (2) | C9—H9 | 0.968 (15) |
| C5—C6 | 1.378 (2) | C11—H11 | 0.9300 |
| C6—C7 | 1.385 (2) | C12—H12 | 0.9300 |
| C7—C8 | 1.4947 (19) | C14—H14 | 0.9300 |
| C8—C9 | 1.5102 (19) | C15—H15 | 0.9300 |
| C9—C10 | 1.4977 (19) | C16—H16A | 0.9600 |
| C10—C11 | 1.3831 (19) | C16—H16B | 0.9600 |
| C10—C15 | 1.375 (2) | C16—H16C | 0.9600 |
| C11—C12 | 1.378 (2) | ||
| O1···C16i | 3.367 (2) | C16···H14 | 2.5100 |
| O3···C4ii | 3.4157 (18) | H3···O1 | 2.5800 |
| O3···C3ii | 3.3841 (18) | H3···O3vi | 2.8300 |
| O1···H3 | 2.5800 | H3···C5iv | 3.0300 |
| O1···H6iii | 2.8500 | H4···O3vi | 2.9000 |
| O1···H9iv | 2.608 (15) | H5···O3x | 2.8200 |
| O1···H8Aiii | 2.6500 | H5···C13x | 3.1000 |
| O1···H16Ai | 2.8600 | H6···O1xi | 2.8500 |
| O2···H11iv | 2.6900 | H6···H8A | 2.4900 |
| O2···H15 | 2.6400 | H8A···O1xi | 2.6500 |
| O2···H16Ci | 2.7800 | H8A···H6 | 2.4900 |
| O3···H3ii | 2.8300 | H8B···C15 | 2.9000 |
| O3···H4ii | 2.9000 | H8B···C2viii | 3.0500 |
| O3···H5v | 2.8200 | H8B···C3viii | 2.9700 |
| C3···C6iv | 3.395 (2) | H9···C2 | 2.915 (14) |
| C3···O3vi | 3.3841 (18) | H9···H11 | 2.3700 |
| C3···C5iv | 3.465 (2) | H9···O1vii | 2.608 (15) |
| C4···O3vi | 3.4157 (18) | H9···C1vii | 2.967 (15) |
| C5···C3vii | 3.465 (2) | H11···H9 | 2.3700 |
| C6···C3vii | 3.395 (2) | H11···O2vii | 2.6900 |
| C16···O1i | 3.367 (2) | H14···C16 | 2.5100 |
| C1···H9iv | 2.967 (15) | H14···H16B | 2.3600 |
| C2···H8Bviii | 3.0500 | H14···H16C | 2.2600 |
| C2···H9 | 2.915 (14) | H15···O2 | 2.6400 |
| C3···H16Avi | 3.0700 | H15···C4viii | 3.0000 |
| C3···H8Bviii | 2.9700 | H15···C5viii | 2.8800 |
| C4···H15viii | 3.0000 | H16A···C3ii | 3.0700 |
| C5···H3vii | 3.0300 | H16A···O1i | 2.8600 |
| C5···H15viii | 2.8800 | H16B···C14 | 2.7600 |
| C13···H5v | 3.1000 | H16B···H14 | 2.3600 |
| C14···H16B | 2.7600 | H16B···C15ix | 3.0700 |
| C14···H16C | 2.7200 | H16C···C14 | 2.7200 |
| C15···H16Bix | 3.0700 | H16C···H14 | 2.2600 |
| C15···H8B | 2.9000 | H16C···O2i | 2.7800 |
| C1—O2—C9 | 119.41 (10) | C4—C3—H3 | 120.00 |
| C13—O3—C16 | 117.70 (12) | C3—C4—H4 | 120.00 |
| O1—C1—O2 | 117.72 (13) | C5—C4—H4 | 120.00 |
| O1—C1—C2 | 124.12 (13) | C4—C5—H5 | 120.00 |
| O2—C1—C2 | 118.15 (11) | C6—C5—H5 | 120.00 |
| C1—C2—C3 | 119.19 (12) | C5—C6—H6 | 120.00 |
| C1—C2—C7 | 120.16 (12) | C7—C6—H6 | 120.00 |
| C3—C2—C7 | 120.63 (12) | C7—C8—H8A | 110.00 |
| C2—C3—C4 | 119.71 (13) | C7—C8—H8B | 110.00 |
| C3—C4—C5 | 119.89 (14) | C9—C8—H8A | 110.00 |
| C4—C5—C6 | 120.77 (14) | C9—C8—H8B | 110.00 |
| C5—C6—C7 | 120.27 (13) | H8A—C8—H8B | 108.00 |
| C2—C7—C6 | 118.72 (12) | O2—C9—H9 | 106.7 (8) |
| C2—C7—C8 | 118.10 (12) | C8—C9—H9 | 110.0 (9) |
| C6—C7—C8 | 123.18 (12) | C10—C9—H9 | 110.0 (9) |
| C7—C8—C9 | 110.17 (11) | C10—C11—H11 | 120.00 |
| O2—C9—C8 | 109.56 (10) | C12—C11—H11 | 120.00 |
| O2—C9—C10 | 107.35 (10) | C11—C12—H12 | 120.00 |
| C8—C9—C10 | 112.99 (11) | C13—C12—H12 | 120.00 |
| C9—C10—C11 | 120.57 (12) | C13—C14—H14 | 120.00 |
| C9—C10—C15 | 121.45 (12) | C15—C14—H14 | 120.00 |
| C11—C10—C15 | 117.85 (13) | C10—C15—H15 | 119.00 |
| C10—C11—C12 | 120.85 (14) | C14—C15—H15 | 119.00 |
| C11—C12—C13 | 120.51 (14) | O3—C16—H16A | 109.00 |
| O3—C13—C12 | 116.22 (13) | O3—C16—H16B | 109.00 |
| O3—C13—C14 | 124.44 (13) | O3—C16—H16C | 109.00 |
| C12—C13—C14 | 119.34 (13) | H16A—C16—H16B | 109.00 |
| C13—C14—C15 | 119.47 (13) | H16A—C16—H16C | 109.00 |
| C10—C15—C14 | 121.98 (13) | H16B—C16—H16C | 109.00 |
| C2—C3—H3 | 120.00 | ||
| C9—O2—C1—O1 | 168.75 (13) | C5—C6—C7—C8 | 178.66 (13) |
| C9—O2—C1—C2 | −12.42 (17) | C2—C7—C8—C9 | 32.06 (16) |
| C1—O2—C9—C8 | 47.27 (15) | C6—C7—C8—C9 | −147.57 (13) |
| C1—O2—C9—C10 | 170.31 (11) | C7—C8—C9—O2 | −55.05 (14) |
| C16—O3—C13—C12 | 175.67 (13) | C7—C8—C9—C10 | −174.68 (11) |
| C16—O3—C13—C14 | −4.8 (2) | O2—C9—C10—C11 | 134.82 (12) |
| O1—C1—C2—C3 | −13.4 (2) | O2—C9—C10—C15 | −49.38 (16) |
| O1—C1—C2—C7 | 164.54 (14) | C8—C9—C10—C11 | −104.28 (15) |
| O2—C1—C2—C3 | 167.82 (12) | C8—C9—C10—C15 | 71.51 (16) |
| O2—C1—C2—C7 | −14.21 (18) | C9—C10—C11—C12 | 175.05 (13) |
| C1—C2—C3—C4 | 178.77 (12) | C15—C10—C11—C12 | −0.9 (2) |
| C7—C2—C3—C4 | 0.81 (19) | C9—C10—C15—C14 | −175.39 (13) |
| C1—C2—C7—C6 | −177.78 (12) | C11—C10—C15—C14 | 0.5 (2) |
| C1—C2—C7—C8 | 2.58 (17) | C10—C11—C12—C13 | 0.8 (2) |
| C3—C2—C7—C6 | 0.17 (18) | C11—C12—C13—O3 | 179.38 (13) |
| C3—C2—C7—C8 | −179.48 (12) | C11—C12—C13—C14 | −0.2 (2) |
| C2—C3—C4—C5 | −1.0 (2) | O3—C13—C14—C15 | −179.72 (13) |
| C3—C4—C5—C6 | 0.2 (2) | C12—C13—C14—C15 | −0.2 (2) |
| C4—C5—C6—C7 | 0.8 (2) | C13—C14—C15—C10 | 0.0 (2) |
| C5—C6—C7—C2 | −1.0 (2) |