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. 2008 Oct 15;64(Pt 11):o2111. doi: 10.1107/S1600536808032625
Bruker KappaAPEXII CCD diffractometer 3302 independent reflections
Radiation source: fine-focus sealed tube 2275 reflections with I > 2σ(I)
graphite Rint = 0.023
Detector resolution: 7.40 pixels mm-1 θmax = 28.8°, θmin = 2.2°
ω scans h = −16→16
Absorption correction: multi-scan (SADABS; Bruker, 2005) k = −19→19
Tmin = 0.980, Tmax = 0.996 l = −9→10
12426 measured reflections