| Bruker SMART CCD area-detector diffractometer | 2551 independent reflections |
| Radiation source: fine-focus sealed tube | 1782 reflections with I > 2σ(I) |
| graphite | Rint = 0.066 |
| φ and ω scans | θmax = 26.0°, θmin = 2.0° |
| Absorption correction: multi-scan (SADABS; Sheldrick, 2001) | h = −30→11 |
| Tmin = 0.834, Tmax = 0.876 | k = −30→29 |
| 20222 measured reflections | l = −21→20 |