| Rigaku SCXmini diffractometer | 2363 independent reflections |
| Radiation source: fine-focus sealed tube | 1607 reflections with I > 2σ(I) |
| graphite | Rint = 0.029 |
| Detector resolution: 13.6612 pixels mm-1 | θmax = 26.0°, θmin = 2.9° |
| ω scans | h = −7→7 |
| Absorption correction: multi-scan (CrystalClear; Rigaku, 2005) | k = −8→8 |
| Tmin = 0.971, Tmax = 0.979 | l = −16→16 |
| 5593 measured reflections |
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