Bruker SMART APEX CCD area-detector diffractometer | 4938 independent reflections |
Radiation source: fine-focus sealed tube | 2362 reflections with I > 2σ(I) |
Monochromator: graphite | Rint = 0.077 |
T = 193(2) K | θmax = 26.0º |
φ and ω scans | θmin = 1.6º |
Absorption correction: multi-scan(SADABS; Bruker, 1998) | h = −9→9 |
Tmin = 0.983, Tmax = 0.987 | k = −15→12 |
13906 measured reflections | l = −31→32 |