| Bruker SMART APEXII CCD diffractometer | 3423 independent reflections |
| Radiation source: fine-focus sealed tube | 2777 reflections with I > 2σ(I) |
| Monochromator: graphite | Rint = 0.020 |
| T = 173(2) K | θmax = 28.3º |
| ω and φ scans | θmin = 2.5º |
| Absorption correction: multi-scan(SADABS; Bruker, 2005) | h = −6→6 |
| Tmin = 0.850, Tmax = 1.000 | k = −26→26 |
| 8526 measured reflections | l = −19→15 |