Bruker SMART APEX area-detector diffractometer | 3374 independent reflections |
Radiation source: fine-focus sealed tube | 2285 reflections with I > 2σ(I) |
Monochromator: graphite | Rint = 0.031 |
T = 298(2) K | θmax = 27.6º |
φ and ω scans | θmin = 2.4º |
Absorption correction: multi-scan(SADABS; Bruker, 2002) | h = −13→13 |
Tmin = 0.604, Tmax = 0.872 | k = −12→8 |
16102 measured reflections | l = −36→29 |