| Rigaku AFC-7R diffractometer | Rint = 0.046 |
| Radiation source: Rigaku rotating anode | θmax = 25.0º |
| Monochromator: graphite | θmin = 2.6º |
| T = 295 K | h = −16→16 |
| ω–2θ scans | k = −6→0 |
| Absorption correction: none | l = −21→10 |
| 2731 measured reflections | 3 standard reflections |
| 2428 independent reflections | every 150 reflections |
| 1482 reflections with I > 2σ(I) | intensity decay: 0.6% |
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