| Bruker SMART CCD area-detector diffractometer | 3203 independent reflections |
| Radiation source: fine-focus sealed tube | 2739 reflections with I > 2σ(I) |
| Monochromator: graphite | Rint = 0.020 |
| Detector resolution: 0 pixels mm-1 | θmax = 25.0º |
| T = 298(2) K | θmin = 2.2º |
| φ and ω scans | h = −11→11 |
| Absorption correction: multi-scan(SADABS; Sheldrick, 1996) | k = −6→12 |
| Tmin = 0.926, Tmax = 0.982 | l = −12→12 |
| 4908 measured reflections |
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