Xcalibur PX κ-geometry diffractometer with CCD Onyx camera	2413 independent reflections
Radiation source: fine-focus sealed tube	2131 reflections with I > 2σ(I)
Monochromator: graphite	Rint = 0.068
T = 100(2) K	θmax = 76.7º
ω and φ scans	θmin = 4.3º
Absorption correction: analytical(CrysAlis RED; Oxford Diffraction, 2006)	h = −38→21
Tmin = 0.21, Tmax = 0.66	k = −4→4
9609 measured reflections	l = −20→26