| Bruker SMART CCD area-detector diffractometer | 5194 independent reflections |
| Radiation source: fine-focus sealed tube | 2351 reflections with I > 2σ(I) |
| Monochromator: graphite | Rint = 0.033 |
| T = 298(2) K | θmax = 25.1º |
| φ and ω scans | θmin = 1.5º |
| Absorption correction: multi-scan(SADABS; Bruker, 2005) | h = −11→11 |
| Tmin = 0.970, Tmax = 0.985 | k = −12→13 |
| 7851 measured reflections | l = −14→17 |