Bruker SMART 1000 CCD area-detector diffractometer | 3280 independent reflections |
Radiation source: fine-focus sealed tube | 2153 reflections with I > 2σ(I) |
Monochromator: graphite | Rint = 0.028 |
T = 298(2) K | θmax = 25.3º |
ω scans | θmin = 2.1º |
Absorption correction: multi-scan(SADABS; Bruker, 2001) | h = −11→11 |
Tmin = 0.932, Tmax = 0.977 | k = −11→11 |
6132 measured reflections | l = −12→12 |