| Enraf–Nonius CAD-4 diffractometer | Rint = 0.0000 |
| Radiation source: fine-focus sealed tube | θmax = 25.3º |
| Monochromator: graphite | θmin = 2.4º |
| T = 294(2) K | h = 0→18 |
| ω/2θ scans | k = 0→9 |
| Absorption correction: ψ scan(North et al., 1968) | l = 0→20 |
| Tmin = 0.978, Tmax = 0.993 | 3 standard reflections |
| 1932 measured reflections | every 120 min |
| 1846 independent reflections | intensity decay: none |
| 905 reflections with I > 2σ(I) |
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