| Bruker SMART APEXII diffractometer | 2065 reflections with I > 2σ(I) |
| Monochromator: graphite | Rint = 0.032 |
| T = 100(2) K | θmax = 26.4º |
| ω scans | θmin = 2.6º |
| Absorption correction: multi-scan(SADABS; Sheldrick, 1996) | h = −13→7 |
| Tmin = 0.614, Tmax = 0.668 | k = −13→12 |
| 6343 measured reflections | l = −11→11 |
| 2298 independent reflections |