| Bruker SMART 1000 CCD diffractometer | 2705 independent reflections |
| Radiation source: fine-focus sealed tube | 2187 reflections with I > 2σ(I) |
| Monochromator: graphite | Rint = 0.022 |
| T = 173(2) K | θmax = 26.0º |
| ω scans | θmin = 1.8º |
| Absorption correction: multi-scan(SADABS; Sheldrick, 2004) | h = −26→23 |
| Tmin = 0.829, Tmax = 0.934 | k = −5→7 |
| 6230 measured reflections | l = −19→28 |